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The Effect of Bromide Process on the Gel Content of Brominated Butyl Rubber

Dong Mimi, Guo Wenli, Li Shuxin, Chang Jinjie, Zhang Tao
Abstract306)      PDF (1515KB)(62)      
 

Gel content has a certain impact on the immanent quality of rubber products and processing performance. Therefore, it is crucial for brominated butyl rubber to control the gel content. Brominated butyl rubber (BIIR) was prepared by solution method and the effect of the brominated process such as bromination temperature, additives, bromination time and bromide agent on the gel content of BIIR was investigated. The results show that the appropriate reaction temperature is conducive to the control of the gel content. Gel content will increase with the increasing of the concentration of time and bromide agent. The additives can lower the gel content.

2016, 29 (2): 23-26. DOI: 10.3969/j.issn.1006-396X.2016.02.005
Screening Study of Weak Alkali Ternary Multisystem
WU Wenxiang, MU Limin,ZHANG Tao, ZOU Jirui
Abstract474)      PDF (1562KB)(290)      
The two surfactants (SS, SHSAHN6) and two polymers (KYPAM, ZLⅡ) compound with Na2CO3 was made, then study on the viscoelasticity of multisystem, evaluate the interfacial tension of multisystem and do physical oil displacement experiments with heterogeneous artificial cores. The optimal multisystem was then selected among various systems as the one to be applied in the field test. The results show that: Along with the increase of shear rate, the viscosity of each multisystem decreases, but the decline phase is not obvious. The elasticity of different systems increases along with the increase of shear rate and the superposition of elasticity points indicate they have good match. Four systems are all achieve ultralow interfacial tension in five minutes, and the steady interfacial tension will remain low. SS is better than SHSAHN6 in decreasing interfacial tension, and the surface tension stability of KYPAM ternary system is much better than ZLⅡternary system. From the perspective of flooding effect evaluation, the chemical flooding recovery of KYPAM ternary system is higher than ZLⅡternary system, the oil displacement efficiency of SS ternary system is better than SHSAHN6 ternary system. 
2013, 26 (4): 66-69. DOI: 10.3969/j.issn.1006396X.2013.04.014